A Convenient Synthesis of 3-Aryl-3-(5,5-dimethyl-3-hydroxy-2-cyclohexene-1-one-2-yl) Propanic Esters Catalyzed by KF-Alumina

Daqing Shi Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

Shujiang Tu Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

Zaisheng Lu Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

Suhui Wang Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

Guiyuan Dai Department of Chemistry, Xuzhou Normal University, Xuzhou, 221009, P. R. China

Abstract

A series of 3-aryl-3-(5,5-dimethyl-3-hydroxy-2-cyclohexene-1-one-2-yl) propanic esters were synthesized by reaction of aromatic aldehydes, 5,5-dimethyl-1,3-cyclohexanedione and isopropylidene malonate in alcohols catalyzed by KF-Al₂O₃. The structure of 4a was determined by X-ray analysis.

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A Convenient Synthesis of 3-Aryl-3-(5,5-dimethyl-3-hydroxy-2-cyclohexene-1-one-2-yl) Propanic Esters Catalyzed by KF-Alumina

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A Convenient Synthesis of 3-Aryl-3-(5,5-dimethyl-3-hydroxy-2-cyclohexene-1-one-2-yl) Propanic Esters Catalyzed by KF-Alumina

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