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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 18
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Original Articles

Synthesis of Neolignan Ocimin and Analogues by Titanium Mediated Coupling of Methoxycinnamyl Alcohols

M. Gaxiola Centro de Graduados e Investigación, Instituto Tecnológico de Tijuana, Apartado Postal 1166, B. C. 22000, Tijuana, México
,
G. V. Rodríguez Centro de Graduados e Investigación, Instituto Tecnológico de Tijuana, Apartado Postal 1166, B. C. 22000, Tijuana, México
,
M. Parra-Hake Centro de Graduados e Investigación, Instituto Tecnológico de Tijuana, Apartado Postal 1166, B. C. 22000, Tijuana, México
&
R. Somanathan Centro de Graduados e Investigación, Instituto Tecnológico de Tijuana, Apartado Postal 1166, B. C. 22000, Tijuana, México
Pages 3423-3430 | Received 01 Apr 1998, Published online: 22 Aug 2006
 
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Abstract

Coupling of Methoxycinnamyl alcohols to form Ocimin, and its 1,6-bisdiaryl-(E)-(E)-hexa-1, 5-diene analogues was effected using McMurry reagents TiCl3/Zn-Cu or TiCl3/LiAlH4. Linear and branched products were obtained with ratios depending on the Titanium reagent used.

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