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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 19
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Original Articles

An Improved Synthetic Preparation of 3-Butenal

Michael T. Crimmins Venable and Kenan Laboratories of Chemistry, The University of North Carolina at Chapel Hill Chapel Hill, North Carolina, 27599-3290
,
Steven J. Kirincich Venable and Kenan Laboratories of Chemistry, The University of North Carolina at Chapel Hill Chapel Hill, North Carolina, 27599-3290
,
Angela J. Wells Venable and Kenan Laboratories of Chemistry, The University of North Carolina at Chapel Hill Chapel Hill, North Carolina, 27599-3290
&
Allison L. Choy Venable and Kenan Laboratories of Chemistry, The University of North Carolina at Chapel Hill Chapel Hill, North Carolina, 27599-3290
Pages 3675-3679 | Received 16 Apr 1998, Published online: 22 Aug 2006
 
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Abstract

A convenient synthesis of 3-butenal from aqueous glyoxal and allyl bromide is described. The preparation readily provides multigram quantities of 3-butenal.

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