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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 1
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Original Articles

α-Chlorination of Ketones with Sodium Chlorite, Mn(acac)3, and Alumina in Dichloromethane

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Pages 131-138 | Received 01 Jul 1997, Published online: 20 Aug 2006
 

Abstract

Chlorination of a variety of aliphatic, alicyclic, and aromatic ketones with a reagent combination of NaClO2 and Mn(acac)3 catalyst can be readily performed in dichloromethane to afford α-chloroketones in good yield under mild and neutral conditions with the aid of chromatographic neutral alumina.

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