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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 28, 1998 - Issue 7
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Original Articles

Synthesis of Diacyl Bisulfides Using a Polymer Supported Reagent

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Pages 1275-1280 | Received 05 Jul 1997, Published online: 15 Aug 2006
 

Abstract

Various diacyl disulfides are prepared easily in high yields from the corresponding acid chlorides under mild and non-aqueous conditions using a polymer supported reagent obtained from elemental sulfur and Amberlyst (OH). The polymeric reagent is regenerable.

Notes

Polymer supported reagent has to be used in the wet form. It will slowly lose its activity if dried.

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