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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 1
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Original Articles

Facile nBu4 NF Mediated Benzylation Of Congested 1,3-Diketones

Pages 117-122 | Accepted 25 Apr 1998, Published online: 17 Sep 2007
 

Abstract

Facile benzylation of 1,3-diketones is mediated by nBu4NF in THF-water. The reaction conditions are mild, the performance is simple, and the yields are high. Importantly, no O-alkylation side reactions or subsequent retro-Claisen C-C-bond cleavage are observed even in sterically congested systems.

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