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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 3
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Original Articles

The Improved Method of Oxidation of 4-Fluoroaniline to 4-Fluoroazobenzene

Xiao-Yang Wang Department of Chemistry, National Laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou, 730000, P. R. China
,
Yu-Lu Wang Department of Chemistry, Henan Normal University, Xinxiang, 453002, China
,
Zi-Yi Zhang Department of Chemistry, National Laboratory of Applied Organic Chemistry, Lanzhou University, Lanzhou, 730000, P. R. China
,
Cai-Lan Wang Department of Chemistry, Henan Normal University, Xinxiang, 453002, China
,
Jian-Ping Li Department of Chemistry, Henan Normal University, Xinxiang, 453002, China
,
Lei Shi Department of Chemistry, Henan Normal University, Xinxiang, 453002, China
&
Zhi-Fang Duan Department of Chemistry, Henan Normal University, Xinxiang, 453002, China
 show all
Pages 481-485 | Received 29 Jul 1998, Published online: 17 Sep 2007
 
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Abstract

The improved method of oxidation of 4-fluoroaniline to 4-fiuoroazobenzene with K3Fe(CN)6/KOH and 2,4,6-tri-tert-butylphenol as catalyst is described for the first time in this paper. This report offers an efficient and rapid method to prepare azobenzene and a possible mechanism is also suggested.

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