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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 10
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Original Articles

First Preparation Of 5-Allyl-1,3-Oxazolidine-2-Thione (Napoleiferin), A Natural Homolog Of 5-Vinyl-1,3-Oxazolidine-2-Thione(Goitrin)

L. Latxague Laboratoire de Chimie Bio-Organique, Université Victor Segalen Bordeaux 2., 146 Rue Léo Saignat F-33076, Bordeaux Cedex, France
&
C. Gardrat Laboratoire de Chimie des Substances Végétales, Institut du Pin, UniversitÉ Bordeaux I, 351 Cours de la Libération F-33405, Talence Cedex, France
Pages 1627-1637 | Accepted 10 Oct 1998, Published online: 17 Sep 2007
 
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Abstract

The preparation of 5-allyl-1.3-oxazolidine-2-thione (napoleiferin) 5 via a practical synthesis of but-3-enal 2 and the key intermediate 1 -aminopent-4-en-2-ol 4 is described for the first time.

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