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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 13
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Original Articles

Direct Synthesis P-Nitrocalix[4]arene from P-tert-Butylcalix[4]arene

Ping-Shan Wang Department of Chemistry, Zhejiang University, Hangzhou, 310027, P. R. of China
,
Rui-Sen Lin Department of Chemistry, Zhejiang University, Hangzhou, 310027, P. R. of China
&
Han-Xing Zong Department of Chemistry, Zhejiang University, Hangzhou, 310027, P. R. of China
Pages 2225-2227 | Accepted 15 Nov 1998, Published online: 17 Sep 2007
 
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Abstract

Calix[4]arene 2 can be directly prepared from p-t-butylcalix[4]arene 1 by concentrated nitric acid or using potassium nitrate and aluminium chloride as a nitrating agent. Product is easily isolated in excellent yield.

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