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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 13
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Original Articles

A Novel Synthesis of 4,6-Dimethyl-2-pyrone from Carbon Dioxide and Mesityl Oxide in the Presence of an Ethylzinc Carbamate

, , &
Pages 2241-2247 | Accepted 11 Nov 1998, Published online: 17 Sep 2007
 

Abstract

The title synthesis, the first example of the CO2 fixation by use of an α, β-unsaturated ketone, has been successfully carried out, most preferably in triethylamine or pyridine at 120-160°C in the presence of ethylzinc diphenylcarbamate.

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