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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 13
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Original Articles

An Efficient Method for Production and Storage of Unstable S-Nitrosothiols Under Mild and Heterogeneous Condition with Sodium Nitrite and Oxalic Acid Dihydrate

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Pages 2277-2280 | Accepted 15 Nov 1998, Published online: 17 Sep 2007
 

Abstract

Thiols can be readily converted to their corresponding nitrosothiols with a combination of oxalic acid and sodium nitrite in t-butanol at room temperature (26-30°C). The reaction mixture could be solidified with decreasing its temperature to, 15°C and was stored for several days without any destruction of the nitrosothiols.

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