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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 13
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Original Articles

Hypervalent Iodine in Synthesis XXXI: Formation of Phosphinimines and Arsinimines by Nitrene Route or Non-Nitrene Route

Wei Ou Department of Chemistry, Hangzhou University, Hangzhou, Zhejiang, 310028, P.R. China
,
Zhi-Gang Wang Department of Chemistry, Hangzhou University, Hangzhou, Zhejiang, 310028, P.R. China
&
Zhen-Chu Chen Department of Chemistry, Hangzhou University, Hangzhou, Zhejiang, 310028, P.R. China
Pages 2301-2309 | Received 11 Dec 1998, Published online: 17 Sep 2007
 
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Abstract

N-suIfonyltriphenylphosphinimines and N-sulfonyltriphenylarsinimines are prepared by the reaction of triphenylphosphine or triphenylarsine under nitrene-producing conditions with I-N ylide (PhI=NSO2R). Triphenylarsinimines can also be generated by a non-nitrene route from triphenylarsine, iodobenzene diacetate, and sulfonamides via triphenylarsine diacetale, Ph3As(OAc)2.

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