Microwave Thermolysis V: A Rapid and Selective Method for the Cleavage of THP Ethers, Acetals and Acetonides Using Clay Supported Ammonium Nitrate “Clayan” in Dry Media

H. M. Meshram Indian Institute of Chemical Technology, Hyderabad, 500 007, India

G. Sumithra Indian Institute of Chemical Technology, Hyderabad, 500 007, India

G. S. Reddy Indian Institute of Chemical Technology, Hyderabad, 500 007, India

Y. S. S. Ganesh Indian Institute of Chemical Technology, Hyderabad, 500 007, India

J. S. Yadav Indian Institute of Chemical Technology, Hyderabad, 500 007, India

Abstract

The deprotection of a variety of tetrahydropyranyl ethers (THP), acetonides and acetals into their parent compounds using clay supported ammonium nitrate “Clayan” under microwave irradiation is described. The eco-friendly nature of the reagent and non solvent conditions are the important features of the procedure.

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Microwave Thermolysis V: A Rapid and Selective Method for the Cleavage of THP Ethers, Acetals and Acetonides Using Clay Supported Ammonium Nitrate “Clayan” in Dry Media

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Microwave Thermolysis V: A Rapid and Selective Method for the Cleavage of THP Ethers, Acetals and Acetonides Using Clay Supported Ammonium Nitrate “Clayan” in Dry Media

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