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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 29, 1999 - Issue 16
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Original Articles

A Facile Preparation of Alkyl Azides from Alkyl Bromides and Sodium Azide Using 18-Crown-6 Ether Doped Clay

Rajender S. Varma Department of Chemistry and Texas Research Institute for Environmental Studies (TRIES), Sam Houston State University, Huntsville, Texas, 77341-2117, U.S.A.
,
Kannan P. Naicker Department of Chemistry and Texas Research Institute for Environmental Studies (TRIES), Sam Houston State University, Huntsville, Texas, 77341-2117, U.S.A.
&
Jason Aschberger Department of Chemistry and Texas Research Institute for Environmental Studies (TRIES), Sam Houston State University, Huntsville, Texas, 77341-2117, U.S.A.
Pages 2823-2830 | Received 02 Feb 1999, Published online: 25 Sep 2007
 
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Abstract

A high yield synthesis of alkyl azides is described from readily accessible alkyl bromides and sodium azide using a recyclable phase transfer catalyst, 18-crown-6 ether impregnated clay.

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