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Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry Volume 10, 1980 - Issue 1
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Original Articles

Facile Synthesis of 57Fe(CO)5

B. Bernard Department of Chemistry, Abilene Christian University, Abilene, Texas
,
L. Daniels Department of Chemistry, Abilene Christian University, Abilene, Texas
,
R. Hance Department of Chemistry, Abilene Christian University, Abilene, Texas
&
B. Hutchinson Department of Geology, University of Oklahoma, Norman, Oklahoma
Pages 1-7 | Received 07 Jun 1979, Accepted 10 Aug 1979, Published online: 13 Dec 2006
 
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Abstract

An improved, one-step synthesis for Fe(CO)5 designed for use with 57Fe is presented. This method allows for easy recovery of the unreacted starting material, requires low pressures, and avoids the use of specialized equipment.

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