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Original Articles

Synthesis and Characterization of Some Phosphine-Boranes and Phosphine- and Phosphite-Cyanoboranes

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Pages 67-75 | Received 04 Jun 1985, Accepted 29 Aug 1985, Published online: 05 Dec 2006
 

Abstract

Phosphine-boranes have been very conveniently prepared in high yields by the reaction of NaBH4 and I2 with the corresponding phosphine in refluxing tetra-hydrofuan. Phosphine- and phosphite-cyanoboranes have been prepared by the reaction of NaBH3CN with I2 with the corresponding phosphine or phosphite in refluxing monoglyme. All these compounds have been characterized by elemental analysis, IR spectra and proton NMR spectra.

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