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Original Articles

Organotin Compounds. I. The Synthesis of Some Dibutyltin and Dibenzyltin Azides and Sulfonates

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Pages 777-793 | Received 09 Jul 1985, Accepted 03 Apr 1986, Published online: 13 Dec 2006
 

Abstract

SUMMARY

The reactions of dibutyltin dichloride and dibenzyltin dichloride with sodium azide, sodium p-toluenesulfonate and silver trifluoromethanesulfonate have been investigated. The products of these reactions include the expected dialkyltin azides and p-toluenesulfonates. In the reactions involving silver trifluoromethanesulfonate, the dialkyltin dichlorides gave only the 1,1,3,3-tetraalkyl-1,3-bis (trifluoromethanesulfonato)- distannoxanes. Other distannoxanes containing the azide and trifluoromethanesulfonato groups attached to tin were also prepared. The infrared spectra and the conductivity characteristics of these compounds are discussed.

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