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Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry Volume 16, 1986 - Issue 9
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Original Articles

The Synthesis of some (η3-Allyl)Dicarbonylthiosemicarbazidohalogenomolybdenum Complexes

Michel J.M. Campbell The School of Chemistry, Thames Polytechnic, Wellington Street, London, SE18 6PF
,
Elizabeth Houghton The School of Chemistry, Thames Polytechnic, Wellington Street, London, SE18 6PF
,
Vernon Rogers The School of Chemistry, Thames Polytechnic, Wellington Street, London, SE18 6PF
&
Paul K. Baker The Department of Chemistry, University College of North Wales, Bangor, LL57 2UW
Pages 1237-1242 | Received 18 Apr 1986, Accepted 24 Jul 1986, Published online: 13 Dec 2006
 
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Abstract

The synthesis of the new complexes [MoX(CO)2(H2NNHCSNH2) (η3-C3H4R)] (R[dbnd]H or Me; X [dbnd] Cl, Br) is described. The procedure involves the reaction of [MoX(CO)2 (NCMe)2(η3-C3H4R)] with thiosemicarbazide in dichloromethane or acetonitrile.

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