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Journal of Coordination Chemistry Volume 62, 2009 - Issue 8
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Original Articles

Synthesis, spectroscopic characterization, and X-ray crystal structure of tris(trimethylsilyl)cyanurate

Nadia E.A. El-Gamel Faculty of Science, Chemistry Department, Cairo University, 12613 Giza, EgyptCorrespondence[email protected]
,
Joerg Brand Chemistry Department, University of Konstanz, PO M736, 78457 Konstanz, Germany
&
Edwin Kroke Institut für Anorganische Chemie, TU Bergakademie Freiberg, leipziger strasse 29, 09596 Freiberg, Germany
Pages 1278-1284 | Received 05 Jun 2008, Accepted 21 Jul 2008, Published online: 29 Jul 2010
 
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Abstract

Tris(trimethylsilyl)cyanurate, C12H27N3O3Si3 (1), has been synthesized and characterized by elemental analysis, IR, Raman, 13C and 29Si NMR, and thermogravimetric methods. The molecular and crystal structure has been determined by single crystal X-ray diffraction. This compound crystallized in space group P63/m (176), Z = 2 with a = 11.017(2), b = 11.017(2), c = 9.676(3) Å; α = 90°, β = 90°, γ = 120°. The geometry of the molecule is compared with tris(trimethylsilyl)cyamelurate.

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