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Journal of Coordination Chemistry Volume 64, 2011 - Issue 15
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Original Articles

Hydrothermal syntheses and crystal structures of two Zn(II) complexes with 1-substituted-1H-[1,2,3]-triazole-4-carboxylic acid

Hong Zhao School of Chemistry and Chemical Engineering, Southeast University, Nanjing 211189, P.R. ChinaCorrespondence[email protected]
,
Jin-Mei Chen School of Chemistry and Chemical Engineering, Southeast University, Nanjing 211189, P.R. China
,
Jin-Rui Lin School of Chemistry and Chemical Engineering, Southeast University, Nanjing 211189, P.R. China
&
Wen-Xiang Wang School of Chemistry and Chemical Engineering, Southeast University, Nanjing 211189, P.R. China
Pages 2735-2745 | Received 13 Sep 2010, Accepted 24 Jun 2011, Published online: 09 Aug 2011
 
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Abstract

Two new Zn(II) complexes, [Zn(L)2(H2O)2] where L is 1-substituted 5-methyl-1H-[1,2,3]-triazole-4-carboxylic acid, have been synthesized and characterized by elemental analysis, FT–IR, and solid-state fluorescent emission spectroscopy. Structures have been established by single-crystal X-ray diffraction, revealing the discrete nature of the complexes in which Zn centers adopt slightly distorted octahedral geometry. In the complexes, the 1-substituted 5-methyl-1H-[1,2,3]-triazole-4-carboxylic acid is bidentate.

Acknowledgments

We gratefully acknowledge the financial support of the National Natural Science Foundation of China (20801012) and the financial support for Young researcher from Southeast University (4007041027).

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