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Journal of Coordination Chemistry Volume 64, 2011 - Issue 21
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Original Articles

Sonochemical synthesis and characterization of a nanostructured 3-D lead(II) coordination polymer with 4-methoxybenzoyltrifluoroacetone

Farzin Marandi Department of Chemistry, Payame Noor University, 19395-4697, Tehran, Islamic Republic of IranCorrespondence[email protected]
,
Vahid Safarifard Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, P.O. Box 14115-4838, Tehran, Islamic Republic of Iran
,
Ali Morsali Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, P.O. Box 14115-4838, Tehran, Islamic Republic of IranCorrespondence[email protected]
&
Hoong-Kun Fun X-ray Crystallography Unit, School of Physics, Universiti Sains Malaysia, 11800USM, Penang, Malaysia
Pages 3781-3791 | Received 13 Jul 2011, Accepted 22 Sep 2011, Published online: 01 Nov 2011
 
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Abstract

Nanoparticles of a 3-D coordination polymer, [Pb2(mbtfa)4] n (1) (Hmbtfa = 4-methoxybenzoyltrifluoroacetone), have been synthesized by a sonochemical method. The nanomaterial was characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy, and elemental analyses. Compound 1 was structurally characterized by single-crystal X-ray diffraction. The structure of 1 shows the compound is triclinic and consists of 3-D polymeric units.

Acknowledgments

Support of this investigation by Payame Noor University and Iran National Science Foundation, INSF is gratefully acknowledged by FM. HKF thanks the Malaysian Government and Universiti Sains Malaysia for the University Golden Goose Fund (Grant No. 1001/PIZIK/811012).

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