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Journal of Coordination Chemistry Volume 66, 2013 - Issue 15
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The construction of two lanthanide coordination polymers based on 5-hydroxyisophthalate and bipyridine

Fen ZhangSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
,
Xiao-Ting HuangSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
,
Yuan-Yuan TianSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
,
Ying-Xin GongSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
,
Xue-Yun ChenSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
,
Jing-Jun LinSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
,
Dong-Sheng LuSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
,
Yan-Lin ZhangSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
,
Rong-Hua ZengSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
&
Sheng-Run ZhengSchool of Chemistry and Environment, South China Normal University, Guangzhou, China
 show all
Pages 2659-2668 | Received 12 Nov 2012, Accepted 28 Mar 2013, Published online: 16 Jul 2013
 
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Abstract

Two lanthanide coordination polymers, [Tm2·(5-IPA)4·(2,2′-Hbipy)2]·3H2O (1, 5-H2IPA = 5-hydroxyisophthalic acid, 2,2′-bipy = 2,2′-bipyridine) and [Er·(5-HIPA)3·(4,4′-bipy)3·(H2O)2]·3H2O (2, 4,4′-bipy = 4,4′-bipyridine), have formed by hydrothermal synthesis. Complex 1 exhibits a 2-D coordination network containing parallelepiped-shaped voids occupied by guest 2′2-bipy molecules. Complex 2 possesses a 1-D linear chain structure. The 1-D chains are linked by 4,4′-bipy molecules to form a 3-D supramolecular framework. IR spectroscopy, elemental analysis, and thermogravimetric analysis were also investigated.

Acknowledgements

This work was financially supported by the Undergraduates’ Innovating Experimentation Project of Guangdong Province, the Undergraduates’ Innovating Experimentation Project of South China Normal University and Natural Science Foundation of Guangdong Province (grant nos. 10451063101004667 and 10451063101006346).

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