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Journal of Coordination Chemistry Volume 70, 2017 - Issue 17
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Articles

Solvent-controlled structural variation from 1D+2D→3D network with coexistence of polycatenation and polythreading to the 2D→3D polythreaded array

Chao ZhangCollege of Chemical Science and Engineering, Qingdao University, Qingdao, China
,
Yue WangCollege of Chemical Science and Engineering, Qingdao University, Qingdao, ChinaCorrespondence[email protected]
,
Yan QiCollege of Chemical Science and Engineering, Qingdao University, Qingdao, China
,
Qun LiCollege of Chemical Science and Engineering, Qingdao University, Qingdao, ChinaCorrespondence[email protected]
&
Zhou LvCollege of Chemical Science and Engineering, Qingdao University, Qingdao, China
Pages 2929-2939 | Received 31 Mar 2017, Accepted 11 Jul 2017, Published online: 05 Sep 2017
 
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Abstract

This article represents two types of entanglements, [Co2(bibp)(BTB)2][Co(bibp)2(H2O)2] (1) and [Co3(bibp)2(H2O)2(BTB)2]·2H2O·2DMF (2) (bibp = 4,4′-bis(1-imidazolyl)biphenyl and H3BTB = 1,3,5-tris(4-carboxyphenyl)benzene), which are 2-D→3-D polycatenated frameworks formed by parallel catenation of 1-D+2-D→2-D polythreaded motifs based on the double-layered sheet penetrated by ribbons of rings (1) and a 2-D→3-D mutual polythreading of three double-layered sheets with dangling arms (2), which is assembled by the same initial materials by simply changing the volume ratio of water/DMF medium.

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