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Journal of Coordination Chemistry Volume 12, 1982 - Issue 1
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Original Articles

THE SYNTHESIS AND PROPERTIES OF SUBSTITUTED TERTIARY BISMUTHINE LIGANDS

Wiliam Levason Department of Chemistry, The University, Southampton, SO9 5NH
,
Baharrudin Sheikh Department of Chemistry, The University, Southampton, SO9 5NH
&
Francis P. McCullough Department of Chemistry, The University, Southampton, SO9 5NH; Dow Chemicals (Texas Division), (I + MR), Freeport, Texas, USA
Pages 53-57 | Received 11 Jan 1982, Published online: 19 Dec 2006
 
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Abstract

The synthesis of functionally substituted (OMe, -NMe2, -SMe) organobismuthine ligands -specifically (o-MeOC6H4)3Bi, (o-MeSC6H4)3Bi, (o-Me2NC6H4)3Bi, (o-MeOC6H4)Ph2Bi, (o-MeSC6H4)Ph2Bi, (o-Me2NC6H4)Ph2Bi, is described. (o-Chlorophenyl)diphenylbismuthine reacts with sodium diphenylstibide (NaSbPh2) to give (o-diphenylstibinophenyl)diphenylbismuthine o-C6H4(SbPh2)(BiPh2). The 1H nmr and mass spectra of these ligands, and of (o-MeC6H4)3Bi and (p-MeC6H4)3Bi are reported and discussed.

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