Separation of Some Monothio-β-Diketonate Chelates by Thin-Layer Chromatography

Daniel T. Haworth Department of Chemistry, Marquette University, Milwaukee, WI, 53233

Diana L. Maas Department of Chemistry, Marquette University, Milwaukee, WI, 53233

Manoranjan Das School of Chemistry University of New South Wales, Kensington, N.S.W., 2033

Abstract

Chromatographic data of nine trifluoromonothio-β-diketonate complexes on silica gel are described. The best single or binary eluent was found to be either aromatic or contained chlorine. In a series of complexes containing the same ligand, the R_F value is related to the geometry of the complex.

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Separation of Some Monothio-β-Diketonate Chelates by Thin-Layer Chromatography

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Separation of Some Monothio-β-Diketonate Chelates by Thin-Layer Chromatography

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