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Original Articles

Application of Iso-Selective Gradient Elution for the Separation of Selected Phthalates

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Pages 3153-3166 | Published online: 23 Oct 2006
 

Abstract

In this paper, the overlapping resolution mapping scheme was applied to the gradient HPLC separation of selected phthalates. The procedure employs a minimum of seven experiments for the determination of the optimum mobile phase gradient for the desired separation. In the present work, solvent systems for iso-selective multisolvent gradient elution were used. The overlapping resolution mapping procedure was found to be a rapid and systematic approach for optimizing HPLC separations.

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