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Separation Science and Technology Volume 51, 2016 - Issue 4
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Chiral Separation Paper

An aspect of selecting resolving agents: The role of differences in molecule length in diastereomeric salt resolutions

Zsolt SzeleczkyDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, HungaryView further author information
,
Sándor SemseyDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, HungaryView further author information
,
Péter BagiDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, HungaryView further author information
,
Balázs FődiDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, HungaryView further author information
,
Ferenc FaiglMTA-BME Organic Chemical Technology Research Group, Hungarian Academy of Sciences, Department of Organic Chemical Technology, Budapest University of Technology and Economics, Budapest, HungaryView further author information
,
Emese PálovicsMTA-BME Organic Chemical Technology Research Group, Hungarian Academy of Sciences, Department of Organic Chemical Technology, Budapest University of Technology and Economics, Budapest, HungaryView further author information
&
Elemér FogassyDepartment of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, HungaryCorrespondence[email protected]
View further author information
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Pages 727-732 | Received 12 May 2015, Accepted 03 Nov 2015, Published online: 21 Feb 2016
 
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ABSTRACT

In the course of 49 individual experiments of diastereomeric salt resolution we have examined the effect of the difference between the racemic and resolving agent molecule lengths on the resolution. We concluded that using resolving agents with the molecule length differing by 3 to 6 from the racemic molecule produces the best result.

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Funding

The above project was supported by the Hungarian Scientific and Research Fund (OTKA K104769). The authors are grateful for the support of Richter Gedeon PhD Scholarship.

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