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Distillation

Simultaneous investigation of hydrodynamic characteristics and column mass recovery of waste water of spearmint produced in a hydro-distillation using RDC extraction column

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Pages 2440-2449 | Received 20 Apr 2018, Accepted 14 Nov 2018, Published online: 03 Dec 2018
 

ABSTRACT

A rotary disk contactor (RDC) has been used to investigate the mass recovery of essential oil (EO) in the waste water from hydro-distillation of the spearmint plant by using n-hexane. Amount of mass recovery indicates a proper performance of the RDC. Results show that an increase in rotor speed, dispersed phase flow rate, and nozzle size lead to the mass recovery enhancement. A new correlation has been developed adopting response surface methodology through a Box–Behnken design for the prediction of the mass recovery as a function of rotor speed, dispersed phase flow rate, and nozzle size.

Nomenclature

N=

Rotor speed (rpm)

dr=

Rotor diameter (m)

ds=

Inner stator diameter (m)

D=

Column diameter (m)

H=

Column height (m)

hc=

Compartment height (m)

di=

Drop size (mm)

Vc=

Superficial velocity of continuous phase (m/s)

Vd=

Superficial velocity of dispersed phase (m/s)

Q=

Volumetric flow rate

ω=

Mass fraction

Mw=

Molecular weight

Subscript

C=

Continuous phase

D=

Dispersed phase

I=

Component number

*=

Final concentration or saturated value of concentration

Greek letters

Φ=

Hold-up

Ρ=

Density (kg/m3)

Σ=

Interfacial tension between two phases (N/m)

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