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Abstract
Oxide-dispersion strengthened (ODS) molybdenum has been characterized using transmission electron microscopy (TEM) to determine the effects of irradiation on material microstructure. This work describes the results-to-date from TEM characterization of unirradiated and irradiated ODS molybdenum. The general microstructure of the unirradiated material consists of fine molybdenum grains (<5 µm average grain size) with numerous low angle boundaries and isolated dislocation networks. ‘Ribbon’-like lanthanum oxides are aligned along the working direction of the product form and are frequently associated with grain boundaries, serving to inhibit grain boundary and dislocation movement. In addition to the ‘ribbons’, discrete lanthanum oxide particles have also been detected. After irradiation, the material is characterized by the presence of non-uniformly distributed large (∼20 to 100 nm in diameter), multi-faceted voids, while the molybdenum grain size and oxide morphology appear to be unaffected by irradiation.
Acknowledgements
The authors thank M.W. Phaneuf of Fibics, Inc. for FIB micromachining and imaging, A.J. Falco and R.T. Pieretti for TEM foil preparation, and D.L. Ward for image analysis.