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International Journal of Environmental Analytical Chemistry Volume 75, 1999 - Issue 1-2
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Original Articles

Analysis of Pesticides in Water Samples Using GC-ECD and GC-MS/MS Techniques

María C. Pablos-Espada Department of Analytical Chemistry, University of Almeria, 04071, Almeria, Spain
,
Francisco J. Arrebola-Liébanas Department of Analytical Chemistry, University of Almeria, 04071, Almeria, Spain
,
Antonia Garrido-frenich Department of Analytical Chemistry, University of Almeria, 04071, Almeria, Spain
&
José L. Martínez-Vidal Department of Analytical Chemistry, University of Almeria, 04071, Almeria, Spain
Pages 165-179 | Received 06 Nov 1998, Accepted 23 Apr 1999, Published online: 27 Oct 2006
 
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Abstract

A pesticide multiresidue method for determining dichlorvos, naled. lindane, diazinon. chlorpyri-fos-methyl, dichlofluanid, chlorpyrifos, folpet, α– and β-endosulfan, endosulfan-sulphate, fen-propathrin and acrinathrin in water samples at the levels required by the EEC Drinking Waters Directive has been developed. The pesticides were selected among the most used during die last 20 years in Almeria (Spain), where there is a high agricultural activity. Solid Phase Extraction (SPE) was selected as extraction method after being compared with Liquid-Liquid Extraction (LLE). Moreover, different gas chromatographic detectors (Electron Capture Detector, ECD; Mass Spectrometer, MS; Tandem Mass Spectrometer, MS/MS) were compared. The best results of repeatability and sensitivity were obtained for ECD and MS/MS.

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