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Phosphorus and Sulfur and the Related Elements Volume 33, 1987 - Issue 1-2
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Original Articles

THE REACTION OF ACETYLACETONE WITH DIALKYLPHOSPHITES: Synthesis of Dialkyl 1-methyl-3-oxo-1-butenyl-phosphonates

Yu-Fen Zhao Institute of Chemistry Academia Sinica, Beijing, China
,
Shou-Zou Wei Institute of Chemistry Academia Sinica, Beijing, China
,
Ai-Teng Song Institute of Chemistry Academia Sinica, Beijing, China
&
Chun Zhai Research Institute of Petroleum Processing, Beijing, China
Pages 53-59 | Received 11 Dec 1986, Accepted 22 Jan 1987, Published online: 19 Dec 2006
 
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Abstract

Acetylacetone and its related compounds were transformed into the dialkyl 1-methyl-1-trimethylsiloxyl-3-oxo-butylphosphonates, which after treatment with trifluoroacetic acid were converted into the dialkyl 1-methyl-3-oxo-1-butenylphosphonates.

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