Publication Cover
Journal of Environmental Science and Health, Part B
Pesticides, Food Contaminants, and Agricultural Wastes
Volume 12, 1977 - Issue 2
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Original Articles

M‐(p‐Nitrobenzyl) pyridine as a spray reagent for the thin‐layer chromatographic detection of dimethyl tetrachloroterphthalate herbicide

Pages 155-161 | Received 20 May 1976, Published online: 21 Nov 2008
 

Abstract

The developed thin‐layer chromatogram of DCPA (Dacthal) is sprayed with 4‐(p‐nitrobenzyl)pyridine chromogenic reagent followed by ammonium carbonate solution. The chromatogram is then heated in an oven at 130°C for 20 minutes. When cool, the chromatogram is sprayed with tetraethylenepentamine reagent. DCPA spots appear blue against a white background. The sensitivity of this test is about 1 μg. The procedure is useful to detect DCPA in water and in soil.

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