181
Views
15
CrossRef citations to date
0
Altmetric
Original Articles

Synthesis and Thermal Properties of Polyimide/BaZrO3 Novel Nanocomposites

, , &
Pages 345-349 | Published online: 27 Feb 2012
 

Abstract

Polyimide/barium zirconate composites (PI/BZO) were successfully synthesized through thermal imidization. In this process, different contents of BZO suspensions (5, 10, 15 vol.%) in poly amic acid (PAA) solution, were imidized by heat treatment to form PI/BZO nanocomposites. The as-synthesized hybrid nanocomposites were characterized using X-ray diffraction (XRD), energy dispersive X-ray spectroscopy (EDX) and scanning electron microscopy (SEM). Nanoparticles of BaZrO3 were dispersed homogeneously in the polyimide matrix. Glass transition temperature, T g , and Heat Capacity were measured by Differential Scanning Calorimetry (DSC). The glass transition temperature of PI/BZO nanocomposites was higher than that for the pure polyimide.

ACKNOWLEDGMENT

The authors are grateful to the council of Iran National Science Foundation and the pooya nanopowders research group for providing financial support to undertake this work.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.