713
Views
9
CrossRef citations to date
0
Altmetric
Original Articles

MAOS of D‐Gluconic Acid, D‐Glucono‐1,4‐ and 1,5‐Lactones, Esters, Hydrazides, and Benzimidazoles ThereofFootnote

, , &
Pages 329-338 | Received 25 Nov 2006, Accepted 22 Jun 2007, Published online: 31 Aug 2007
 

Microwave‐assisted organic synthesis (MAOS) of D‐gluconic acid can be efficiently done by oxidation of D‐glucose with bromine water, upon irradiation with microwave (MW). It was also used for the conversion of D‐gluconic acid to ethyl D‐gluconate, D‐glucono‐1,4‐ and 1,5‐lactones, gluconyl hydrazide, and gluconyl phenylhydrazide in yields comparable to those obtained by conventional methods, but in much shorter times. A convenient microwave‐mediated condensation of D‐gluconic acid with o‐phenylenediamines provided the respective acyclonucleoside benzimidazole in short time and good yield.

Notes

A. I. Atta is on leave from Faculty of Medical Sciences, Al-Hodiedah University, Yemen.

Reprints and Corporate Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

To request a reprint or corporate permissions for this article, please click on the relevant link below:

Academic Permissions

Please note: Selecting permissions does not provide access to the full text of the article, please see our help page How do I view content?

Obtain permissions instantly via Rightslink by clicking on the button below:

If you are unable to obtain permissions via Rightslink, please complete and submit this Permissions form. For more information, please visit our Permissions help page.