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Allylic carbonates reacted with carbohydrates having a free anomeric hydroxyl group in the presence of a catalytic amount of palladium(0) giving the unsaturated O-glycosides under neutral conditions with excellent yields. In the mannofuranose and ribofuranose series, the reaction was stereospecific leading only to the α and the β anomers respectively, although a mixture of α and β anomers was obtained in the glucopyranose series.
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