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Phase and Microstructural Characterization of Iron Ore Pellet and their Relation with Cold Crushing Strength Test

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ABSTRACT

In the production of the pellets, phase identification for specific sintering condition is of prime importance in understanding the basis for the production and the required properties. The application of a methodology involving optical and scanning electron microscope equipped with an EBSD opened a broad possibility to establish a base for the relationship between heat-treated pellet microstructural features and cold crushing strength. The first results from the conjoined application of these techniques show that the cold crushing strength of the pellet increase with the decrease of porosity, the appearance of the fayalite, as well as the presence of magnetite-unoxidized.

Acknowledgments

We are thankful to the Laboratory of Microscopy and Microanalysis (MICROLAB), to the Vale pilot plant (Tubarão Complex).

Funding

The financial support of the Fundação de Amparo a Pesquisa do Estado de Minas Gerais (FAPEMIG-APQ-01054) and Vale S.A. is gratefully acknowledged.

List of abbreviations

Abbreviations=

Names

2CF=

dicalcium ferrites

B2=

basicity (CaO/SiO2)

Ca2Si2O6=

dicalcium silicate

CaMgSi2O6=

calcium-magnesium silicate

CCS=

cold crushing strength

CF=

calcium ferrites

CO=

core

DR=

direct reduction process

EBSD=

electron backscatter diffraction

EBSP=

electron backscatter diffraction patterns

Fa=

fayalite

Hem=

hematite

HPGR=

High Pressure Grinding Rolls

IN=

inner mantle

Mag=

magnetite

Mag unoxidized=

magnetite-unoxidized

Mfr=

magnesioferrite

OM=

outer mantle

pO2=

oxygen partial pressure

Qz=

quartz

SEM=

scanning electron microscope

SFCA=

silico-ferrite of calcium and aluminum

SH=

shell

Wus=

wüstite

Additional information

Funding

The financial support of the Fundação de Amparo a Pesquisa do Estado de Minas Gerais (FAPEMIG-APQ-01054) and Vale S.A. is gratefully acknowledged.

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