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High Pressure Research
An International Journal
Volume 20, 2001 - Issue 1-6
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Original Articles

Development of porous silica production by hydrothermal method

, , , , &
Pages 307-310 | Received 10 Jan 2000, Accepted 25 Feb 2000, Published online: 19 Aug 2006
 

Abstract

A new process for porous silica production has been developed using a hydrothermal method. Hydrothermally synthesized calcium silicate was used as the starting material in this study, which was produced from a mixture of Ca(OH)2 and amorphous silica (white carbon) under hydrothermal conditions of 140°C and 0.4 MPa, for 8 hours. The calcium silicate was subsequently treated with an acid solution, facilitating the leaching of Ca ions. After washing with pure water, the multant Ca2+ -free silica powder was allowed to dry. The Ca2+ -free silica powder was found to have an amorphous structure, with 0.9 ml/g pore volume, up to 610m2/g BET specific surface area, and an average 5 ∼ 8 nm pore size. Our hydrothermal process is simple and low cost, and is anticipated to have numerous applications to the petrochemical industry.

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