The high-pressure synthesis of chiral N, N′-dimethyl diazacoronands derived from L- and D-tartaric acid

P. Sałański Institute of Organic Chemistry, Polish Ac Sci, 01-224, Warsaw, Poland

R. Ostaszewski Institute of Organic Chemistry, Polish Ac Sci, 01-224, Warsaw, Poland

J. Jurczak Institute of Organic Chemistry, Polish Ac Sci, 01-224, Warsaw, Poland; Department of Chemistry, University of Warsaw, 02-093, Warsaw, Poland

Abstract

Three enantiomeric pairs of N, N′-dimethyl diazacoronands derived from L- and D-tartaric acid were synthesized by the high-pressure double-quaternization reaction. ¹H, ¹³C NMR and MS techniques were used for structure assignments.

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The high-pressure synthesis of chiral N, N′-dimethyl diazacoronands derived from L- and D-tartaric acid

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The high-pressure synthesis of chiral N, N′-dimethyl diazacoronands derived from L- and D-tartaric acid

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