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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 158, 2000 - Issue 1
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Original Articles

OXIDATIVE DEPROTECTION OF TRIMETHYLSILYL ETHERS TO CARBONYL COMPOUNDS WITH PdCI2(PhCN)2-CrO3 AND CLAY-BIS(TRIMETHYLSILYL) CHROMATE IN SOLVENTLESS SYSTEM

Majid M. Heravi Chemistry & Chemical Engineering Research Center of Iran, P.O. Box 14335-186, Tehran, Iran
,
Dariush Ajami Chemistry & Chemical Engineering Research Center of Iran, P.O. Box 14335-186, Tehran, Iran
,
Kioumars Aghapoor Chemistry & Chemical Engineering Research Center of Iran, P.O. Box 14335-186, Tehran, Iran
&
Mitra Ghassemzadeh Chemistry & Chemical Engineering Research Center of Iran, P.O. Box 14335-186, Tehran, Iran
Pages 151-156 | Received 06 Jul 1999, Published online: 04 Oct 2006
 
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Abstract

A simple and selective oxidative deprotection of trimethylsilyl ethers to carbony1 compounds is described that occurs on PdCl2(PhCN)2-CrO3 and bis(trimethylsily1) chromate under solvent free conditions and is expedited by microwave irradiation.

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