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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 161, 2000 - Issue 1
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Original Articles

PHASE TRANSFER SYNTHESIS OF SYMMETRICAL DI-TERMINALLY PERFLUORINATED ALKYL TRITHIOCARBONATES

C. Naud Luboratoire Organisation moléculaire, Université de Montpellier II, Evolution et matériaux fluorés, UPRESA CNRS 5073, F, 34095, Montpellier Cedex 05, France
,
P. Calas Luboratoire Organisation moléculaire, Université de Montpellier II, Evolution et matériaux fluorés, UPRESA CNRS 5073, F, 34095, Montpellier Cedex 05, France
,
H. Blancou Luboratoire Organisation moléculaire, Université de Montpellier II, Evolution et matériaux fluorés, UPRESA CNRS 5073, F, 34095, Montpellier Cedex 05, France
&
A. Commeyras Luboratoire Organisation moléculaire, Université de Montpellier II, Evolution et matériaux fluorés, UPRESA CNRS 5073, F, 34095, Montpellier Cedex 05, France
Pages 29-38 | Received 22 Sep 1999, Published online: 04 Oct 2006
 
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Abstract

Symmetrical di-terminally perfluorinated alkyl trithiocarbonates having the formula [F(CF2)n(CH2)mS]2CS (n = 4,6,8 m = 2 and n = 6,8 m = 11) were prepared in good yield under phase-transfer catalytic conditions starting from perfluoroalkyl alkyl iodides F(CF2)n(CH2)mI.

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