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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 176, 2001 - Issue 1
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Original Articles

Microwave Induced and Photocatalyzed Hydrophosphorylation Reactions of Perfluoroolefins

D. K. Rohrbaugh US. Army, Edgewood Chemical Biological Center, APG, MD, 21010
,
F. R. Longo Geo-Centers, Inc., PO. Box 68 Gunpowder Branch, APG, MD, 21010
,
H. D. Durst US. Army, Edgewood Chemical Biological Center, APG, MD, 21010
&
S. Munavalli Geo-Centers, Inc., PO. Box 68 Gunpowder Branch, APG, MD, 21010
Pages 201-214 | Received 08 May 2001, Accepted 22 May 2001, Published online: 23 Oct 2006
 
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Abstract

Microwave induced and UV-catalyzed hydrophosphorylation reactions of perfluoroolefins with hydrogen dimethylphosphonate have been examined and found to furnish hydrophosphorylated compounds among other products. This communication attempts to rationalize the formation of compounds and their GC-MS characterization.

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