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A combination of P2O5 and SiO2 was used for an efficient conversion of aldehydes to their corresponding acylals with excellent yields at room temperature under mild conditions.
Yazd University, Bu-Ali Sina University, Kashan University, is gratefully acknowledged for financial support, we also thank Mr. F. Fallah and Mr. H. Babazadeh for their help.
Dedicated to our teacher, professor Abdolhossein Rustaiyan, on the occasion of his seventy-fifth birthday.
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