MICROWAVE SYNTHESIS OF TRICHLORFON AND ITS ANALOGUES: Phosphorus, Sulfur, and Silicon and the Related Elements: Vol 179, No 11

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Abstract

The synthesis of dialkyl-(2,2,2-trichloro-1-Hydroxyethyl) phosphonates using dialkyl hydrogen phosphite and chloral hydrate under solvent-free condition by microwave irradiation is reported. The products were chrachetrized using ¹H NMR, ¹³C NMR, and ³¹P NMR spectroscopy.

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Notes

*Based on the ³¹P NMR of crude reaction mixture.

**450 W.

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MICROWAVE SYNTHESIS OF TRICHLORFON AND ITS ANALOGUES

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MICROWAVE SYNTHESIS OF TRICHLORFON AND ITS ANALOGUES

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