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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 182, 2007 - Issue 1
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Original Articles

TiCl4-Catalyzed Efficient One-Pot Synthesis of α α-Amino Phosphonates

Y. Thirupathi Reddy Department of Chemistry, National Institute of Technology, Warangal, India
,
P. Narsimha Reddy Department of Chemistry, National Institute of Technology, Warangal, India
,
B. Sunil Kumar Department of Chemistry, National Institute of Technology, Warangal, India
,
Pradeep Rajput Department of Chemistry, National Institute of Technology, Warangal, India
,
N. Sreenivasulu Department of Chemistry, National Institute of Technology, Warangal, India
&
B. Rajitha Department of Chemistry, National Institute of Technology, Warangal, India
Pages 161-165 | Received 07 Apr 2006, Accepted 06 Jun 2006, Published online: 01 Feb 2007
 
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Abstract

α-Aminophosphonates are synthesized by three-component condensation of aldehydes, amines, and trimethylphosphite in acetonitrile by using TiCl4 as catalyst. Compared to conventional methods, this new method consistently has advantages, including excellent yields, short reaction times, and mild reaction conditions.

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Related Research Data

A simple protocol for the synthesis of α-substituted phosphonates
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Source: Informa UK Limited

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