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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 184, 2009 - Issue 11
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Original Articles

Synthesis of New Benzoxaphosphole Derivatives from the Reaction of Dialkylphosphonates and Trisdialkylaminophosphines with 2,6-Bis(benzylidene)cyclohexanones

Mona H. N. Arsanious National Research Centre, Dokki, Cairo, Egypt
,
Nahed K. El-Din National Research Centre, Dokki, Cairo, Egypt
&
Leila S. Boulos National Research Centre, Dokki, Cairo, Egypt
Pages 2813-2826 | Received 11 Aug 2008, Accepted 22 Oct 2008, Published online: 03 Nov 2009
 
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Abstract

The reaction of 2,6-bis(benzylidene)cyclohexanones with dialkylphosphonates and tris(dialkylamino)phosphines afforded the new benzoxaphosphole derivatives (5a–5d) and (9a–9f). The biological activity of the newly synthesized compounds was also examined. Possible reaction mechanisms are considered, and the structural assignments are based on analytical and spectroscopic results. The structure of the new benzoxaphosphole 5a was confirmed by a single crystal X-ray determination.

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