Monitoring the Phosphorylation of Phenol with Diethyl Chlorophosphate in Aqueous Medium in the Presence of Sodium Hydroxide by in Situ Fourier Transform Infrared Spectroscopy

György Keglevich Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary

Réka Eszter Puskás Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary

Alajos Grün Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary; Research Group of the Hungarian Academy of Sciences at the Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary

István Csontos Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary

Abstract

In situ Fourier transform IR spectroscopy has been found to be an appropriate tool for monitoring the title reaction resulting in the formation of diethyl phenylphosphate.

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Acknowledgments

The authors are grateful for the OTKA (T067679) support of this work.

Notes

^a Shoulder.

^b A broad signal results from ν_P˭O/ν_P–O–C (aryl) vibrations.

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Monitoring the Phosphorylation of Phenol with Diethyl Chlorophosphate in Aqueous Medium in the Presence of Sodium Hydroxide by in Situ Fourier Transform Infrared Spectroscopy

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Monitoring the Phosphorylation of Phenol with Diethyl Chlorophosphate in Aqueous Medium in the Presence of Sodium Hydroxide by in Situ Fourier Transform Infrared Spectroscopy

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