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Original Articles

Synthesis and Structure of N-[(3Z)-2,2-Di-tert-Butyl-2λ5-Indeno[1,2-D] [1,2]Azaphosphol-3(8H)-Ylidene]-P,P-di-tert-butylphosphinous Amide

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Pages 1278-1283 | Received 24 May 2012, Accepted 06 Jun 2012, Published online: 06 Aug 2012
 

Abstract

The title compound has been obtained from the one-pot reaction of benzene-1,2-dicarbonitrile with NaH followed by addition of two equivalents of tBuPCl2. The compound is obtained as an orange-red solid in good yield and has been characterized by spectroscopic and analytical methods including the determination of the molecular structure by single-crystal X-ray techniques.

GRAPHICAL ABSTRACT

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