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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 188, 2013 - Issue 1-3: 19th International Conference on Phosphorus Chemistry (ICPC-2012) Rotterdam, 8–12 July, 2012
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Original Articles

Synthesis, Characterization, and Activity of Cyclotriphosphazene-Cyclene Conjugates

Jin-Hui Wang Department of Chemistry, Key Laboratory of Chemical Biology and Organic Chemistry of Henan Province, Zhengzhou University, Zhengzhou, 450052, China
,
Cui-Cui Wang Department of Chemistry, Key Laboratory of Chemical Biology and Organic Chemistry of Henan Province, Zhengzhou University, Zhengzhou, 450052, China
,
Di Zhang Department of Chemistry, Key Laboratory of Chemical Biology and Organic Chemistry of Henan Province, Zhengzhou University, Zhengzhou, 450052, China
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Cun-Jiang Liu Department of Chemistry, Key Laboratory of Chemical Biology and Organic Chemistry of Henan Province, Zhengzhou University, Zhengzhou, 450052, China
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Yong Ye Department of Chemistry, Key Laboratory of Chemical Biology and Organic Chemistry of Henan Province, Zhengzhou University, Zhengzhou, 450052, China; Department of Chemistry, Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology (Ministry of Education), Tsinghua University, Beijing, 100084, China
&
Yufen Zhao Department of Chemistry, Key Laboratory of Chemical Biology and Organic Chemistry of Henan Province, Zhengzhou University, Zhengzhou, 450052, China; Department of Chemistry, Key Laboratory of Bioorganic Phosphorus Chemistry and Chemical Biology (Ministry of Education), Tsinghua University, Beijing, 100084, China; Department of Chemistry, Key Laboratory for Chemical Biology of Fujian Province, Xiamen University, Xiamen, 361005, China
Pages 54-58 | Received 05 Aug 2012, Accepted 15 Oct 2012, Published online: 08 May 2013
 
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Abstract

Two novel cyclotriphosphazene derivatives were synthesized from hexachloro cyclotriphosphzene. Their structures were characterized by 1H, 31P, and 13C NMR spectroscopy as well as by IR spectroscopy and electrospray ionization-mass spectrometry (ESI-MS). The Zn complex of 4d was effective in hydrolytic DNA cleavage reactions.

GRAPHICAL ABSTRACT

Acknowledgments

This work was financially supported by the NSFC (Nos. 20972143, 20972130) and the Program for New Century Excellent Talents in University (NCET-11–0950).

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