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Original Articles

P,P,P-Trihalobenzo-1,3,2-Dioxaphopholes in the Reaction with Aliphatic Acetylenes and Diacetylenes: Synthesis of New Phosphacoumarins

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Pages 200-204 | Received 14 Sep 2012, Accepted 22 Oct 2012, Published online: 08 May 2013
 

Abstract

Bis(benzo[e]-1,2-oxaphosphinin-2-oxid-4(7)-yl)butane (-benzene) derivatives were synthesized for the first time both on the basis of reactions of diacetylene with P,P, P-trihalobenzo-1,3,2-dioxaphopholes and on the basis of reactions of bis(P,P,P-trihalobenzo-1,3,2-dioxaphosphol-5-yl)bytane (-benzene) with phenylacetylene.

GRAPHICAL ABSTRACT

Acknowledgments

The work was supported by the Russian Foundation for Basic Research (grant No. 10-03-00525a).

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