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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 190, 2015 - Issue 3
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Original Articles

Synthesis and Crystal Structure of Triethylammonium 2,4,14,16-Tetrachlorodibenzo[g,j][1,3,6,12]Tetraoxacyclo-Tetradecane-2-Phosphorodithioate

Xiao Mei ZhangDepartment of Applied Chemistry, China Agricultural University, Beijing, 100193, People's Republic of China;College of Chemical and Engineering, Anhui University of Science and Technology, Huainan, 232001, Anhui, People's Republic of China
,
Yan Hong DongDepartment of Applied Chemistry, China Agricultural University, Beijing, 100193, People's Republic of China
,
Wan Yi ChenDepartment of Applied Chemistry, China Agricultural University, Beijing, 100193, People's Republic of China
&
Dao Quan WangDepartment of Applied Chemistry, China Agricultural University, Beijing, 100193, People's Republic of ChinaCorrespondence[email protected]
Pages 310-314 | Received 08 Apr 2014, Accepted 24 Jun 2014, Published online: 06 Jan 2015
 
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GRAPHICAL ABSTRACT

Abstract

Triethylammonium 2,4,14,16-tetrachlorodibenzo[g,j][1,3,6,12]tetraoxacyclotetradecane-2-phosphorodithioate was synthesized from bis(3,5-dichloro-2-hydroxyethoxyphenyl)methane by a two-step one-pot sequence. Its structure was confirmed by 1H, 13C, and 31P NMR spectra, and elemental analysis. The X-ray diffraction analysis indicated that the molecules of the compound form an inclusion complex with chloroform molecules outside the phosphorus-containing macrocycle in the ratio of 1:2.

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